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Article << Previous     |     Next >>   Contents Vol 62(9)

Structures and Suzuki-Coupling of N-Heterocyclic Carbene Complexes of PdII with Coordinated Solvent and PPh3

Swee Kuan Yen A, Lip Lin Koh A, Han Vinh Huynh A, T. S. Andy Hor A B

A Department of Chemistry, National University of Singapore, Kent Ridge, 117543, Singapore.
B Corresponding author. Email: andyhor@nus.edu.sg
 
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Abstract

A series of mononuclear N,N-heterocyclic carbene (NNHC) complexes of PdII with mixed ligands of 1,3-dibenzylbenzimidazoly-2-ylidene and solvate (dimethyl sulfoxide, CH3CN, N,N-dimethylformamide, and pyridine) or PPh3 were prepared and characterized by X-ray single-crystal diffraction analysis. They are more active in the Suzuki–Miyaura coupling of selected aryl bromides than their N,S-heterocyclic carbene (NSHC) analogues.

   
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