
%0 Journal Article
%A Edwards, A. J. 
%A Wenger, E. 
%T Simple Method for the Handling of Crystals at Low Temperature: Application to the X-Ray Structure Determination of Bu<emph type="7"><emph type="2">t</emph></emph><emph type="8">2</emph>P(=NSiMe<emph type="8">3</emph>)NHSiMe<emph type="8">3</emph> and [Bu<emph type="7"><emph type="2">t</emph></emph><emph type="8">2</emph>P(NSiMe<emph type="8">3</emph>)<emph type="8">2</emph>]Li&#183;(thf)<emph type="8">2</emph>
%J Australian Journal of Chemistry
%D 2002/07/09
%V 55
%N 4
%P 249-252
%K 
%R https://doi.org/10.1071/CH02016
%U https://www.publish.csiro.au/paper/CH02016 
%X Crystals of the very soluble iminophosphonamide species But2P(=NSiMe3)NHSiMe3 (1) and [But2P(NSiMe3)2]Li·(thf)2 (2) have been obtained and were mounted at dry-ice temperature using a propan-2-ol matrix for X-ray data collection at 100 K. This very simple method for handling the crystals at low temperature is described together with the resulting molecular structures of (1) and (2). 
