
%0 Journal Article
%A Brice, MD 
%A Penfold, BR 
%A Robinson, WT 
%T Crystal and molecular structure of 4&#945;-t-Butylcyclohexane-1&#946;,2&#946;-diol
%J Australian Journal of Chemistry
%D 1972/10/01
%V 25
%N 10
%P 2117-2124
%K 
%R https://doi.org/10.1071/CH9722117
%U https://www.publish.csiro.au/paper/CH9722117 
%X The crystal and molecular structure of 4&#945;-t-butylcyclohexane-1&#946;,2,&#946;-diol, C10H20O2, has been determined by X-ray diffraction methods. The compound crystallizes in the triclinic space group Pi with 4 molecules in a unit cell of dimensions a = 12.268, b = 15.921, c = 6.322Å, &#945; = 82.53, &#946; = 114.45, &#947; = 111.13°. The intensity data were measured by counter methods using Cu K&#945; radiation; the structure was solved by means of the tangent formula, and was refined using full matrix least-squares techniques to a final R-factor of 0.063 for 1199 reflections. The crystal structure consists of two sets of crystallographically non-equivalent molecules hydrogen-bonded to form discrete chains parallel to the c axis. The cyclohexane rings are in the chair conformation. 
