
TY  - JOUR
A1  - Collins, DJ 
A1  - Hetherington, JW 
A1  - Swan, JM 
T1  - Organophosphorus compounds. XV. Synthesis of 2-Ethoxy-1-methyl-1,2-azaphospholidine 2-oxide
JF  - Australian Journal of Chemistry
JO  - Aust. J. Chem.
Y1  - 1974
VL  - 27
IS  - 8
SP  - 1759
EP  - 1765
KW  - 
UR  - https://doi.org/10.1071/CH9741759 
N2  - The reaction of diethyl 3-bromopropylphosphonate with phosphorus pentachloride in carbon tetrachloride gave ethyl 3-bromopropylphosphonochloridate, which upon reaction with anhydrous methylamine at -15º gave ethyl N-methyl-P-3-bromopropylphosphonamidate. Treatment of this phosphonamidate with sodium hydride in boiling xylene gave 2-ethoxy-1-methyl-l,2-azaphospholidine 2-oxide. Some other possible routes to this compound were investigated. 
ER  -

