
%0 Journal Article
%A Raston, CL 
%A White, AH 
%A Willis, AC 
%T Crystal structure of Tris(ethane-1,2-diamine)nickel(II) diperchlorate monohydrate
%J Australian Journal of Chemistry
%D 1978/02/01
%V 31
%N 2
%P 415-418
%K 
%R https://doi.org/10.1071/CH9780415
%U https://www.publish.csiro.au/paper/CH9780415 
%X The crystal structure of the title compound, [Ni(en)3] (ClO4)2,H2O, has been determined from single-crystal X-ray diffraction data at 295(1) K and refined by least squares to a residual of 0.093 for 1400 'observed' reflections. Crystals are orthorhombic, P bca, a 17.043(7), b 15.922(6), c 13.496(5) &#506;, Z 8. The precision of the structure determination is adversely affected by very high perchlorate thermal motion. <Ni-N> is 2.13 &#506;. 
