
TY  - JOUR
A1  - Raston, CL 
A1  - White, AH 
A1  - Willis, AC 
T1  - Crystal structure of Tris(ethane-1,2-diamine)nickel(II) diperchlorate monohydrate
JF  - Australian Journal of Chemistry
JO  - Aust. J. Chem.
Y1  - 1978
VL  - 31
IS  - 2
SP  - 415
EP  - 418
KW  - 
UR  - https://doi.org/10.1071/CH9780415 
N2  - The crystal structure of the title compound, [Ni(en)3] (ClO4)2,H2O, has been determined from single-crystal X-ray diffraction data at 295(1) K and refined by least squares to a residual of 0.093 for 1400 'observed' reflections. Crystals are orthorhombic, P bca, a 17.043(7), b 15.922(6), c 13.496(5) &#506;, Z 8. The precision of the structure determination is adversely affected by very high perchlorate thermal motion. <Ni-N> is 2.13 &#506;. 
ER  -

