
%0 Journal Article
%A Bottomley, GA 
%A Carter, AM 
%A Engelhardt, LM 
%A Lincoln, FJ 
%A Patrick, JM 
%A White, AH 
%T Crystal structure of Bis(8-hydroxyquinolinium) chloride tetrachloroferrate(III), a hydrogen chloride vapour pressure reference source?
%J Australian Journal of Chemistry
%D 1984/04/01
%V 37
%N 4
%P 871-877
%K 
%R https://doi.org/10.1071/CH9840871
%U https://www.publish.csiro.au/paper/CH9840871 
%X The crystal structure of the title compound, [C9H8NO]2[FeCl4]C1, has been determined by single-crystal X-ray diffraction methods at 295 K and refined by least squares to a residual of 0.043 for 2415 independent 'observed' reflections. Crystals are triclinic, P1, a 14.243(5), b 10.177(3), c 7.583(3) Å, &#945; 84.71(3), &#946; 86.96(3), &#947; 86.50(3º, Z 2. The organic moiety is protonated at the nitrogen atom, with the discrete chloride ions hydrogen-bonded in lattice tunnels; this offers a rationale for the finite but small hydrogen chloride partial pressure at room temperature. 
