
TY  - JOUR
A1  - Bottomley, GA 
A1  - Carter, AM 
A1  - Engelhardt, LM 
A1  - Lincoln, FJ 
A1  - Patrick, JM 
A1  - White, AH 
T1  - Crystal structure of Bis(8-hydroxyquinolinium) chloride tetrachloroferrate(III), a hydrogen chloride vapour pressure reference source?
JF  - Australian Journal of Chemistry
JO  - Aust. J. Chem.
Y1  - 1984
VL  - 37
IS  - 4
SP  - 871
EP  - 877
KW  - 
UR  - https://doi.org/10.1071/CH9840871 
N2  - The crystal structure of the title compound, [C9H8NO]2[FeCl4]C1, has been determined by single-crystal X-ray diffraction methods at 295 K and refined by least squares to a residual of 0.043 for 2415 independent 'observed' reflections. Crystals are triclinic, P1, a 14.243(5), b 10.177(3), c 7.583(3) Å, &#945; 84.71(3), &#946; 86.96(3), &#947; 86.50(3º, Z 2. The organic moiety is protonated at the nitrogen atom, with the discrete chloride ions hydrogen-bonded in lattice tunnels; this offers a rationale for the finite but small hydrogen chloride partial pressure at room temperature. 
ER  -

