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Journal of Australian Energy Producers
RESEARCH ARTICLE

Implications of thin laminations on pore structure of marine shale reservoir: Goldwyer Formation case study from Western Australia

Muhammad Atif Iqbal A C , Reza Rezaee A , Gregory Smith B and Partha Pratim Mandal A
+ Author Affiliations
- Author Affiliations

A Department of Petroleum Engineering, Western Australian School of Mines: Minerals, Energy and Chemical Engineering, Curtin University, 26 Dick Perry Avenue, Kensington, WA 6151, Australia.

B Department of Applied Geology, West Australian School of Mines, Curtin University, Perth, Australia.

C Corresponding author. Email: m.atifiqbal16@gmail.com

The APPEA Journal 61(1) 205-215 https://doi.org/10.1071/AJ20025
Submitted: 17 December 2020  Accepted: 17 February 2021   Published: 2 July 2021

Abstract

The pore structure of a shale reservoir is a major control on hydrocarbon potential, yet shale pore systems are complex and affected by various factors. This paper focuses on the differences in pore structure between thinly laminated and massive black shale (MBSh) beds in the Ordovician Goldwyer-III shale, Canning Basin, Western Australia. A multiscale approach included image logs, core descriptions, thin sections, scanning electron microscope and X-ray diffraction analysis with low-pressure nitrogen and carbon dioxide gas adsorption tests. The results indicate that the Goldwyer shale comprises laminated beds of quartz silt and shale with thin beds of organic-rich clay, plus minor interbedded carbonate bands or concretions. The pore types are subjected to rock type, and the thinly laminated shale (LSh) is enriched in intergranular and intragranular pores. In contrast, the MBSh mainly comprises organic matter pores. The LSh is slightly enriched in mesopores but has negligible micropores. The mesopores are wedge-shaped and associated with an inorganic matrix of clay and pyrite. In comparison, the MBSh contains both mesopores and micropores. These pores are slit-like and related to organic matter and clay. The clay content and total organic carbon fluctuations control the development of mesopores and micropores in both the laminated and MBSh beds in the Goldwyer-III shale. The MBSh layers are suggested as the most important rock types for fluid flow via pore systems due to higher total pore volume, specific surface area and gas adsorption capacity.

Keywords: Western Australia, Goldwyer Formation, Goldwyer-III shale, shale reservoir, laminations, massive beds, pore structure, shale pore systems, Canning Basin, hydrocarbon potential, Ordovician.

Mr Muhammad Atif Iqbal is currently a PhD Candidate in Western Australia School of Mines (WASM), Curtin University. His PhD research is focused on the high-resolution mineralogical and petrophysical characterisation of shale reservoirs. He is solving a research problem about heterogeneity understanding through multiscale (analytical and machine learning-based) rock typing and its influence on the total gas content of marine shale reservoirs. This research is timely and will be helpful for accurate reserve estimations in the shale. He has more than five years of industry and research experience as a Geoscientist for petroleum and mineral exploration companies. His expertise lies in core logging, petrophysics, geological and geochemical characterisation and well logs analysis. He has won different research scholarships throughout his academic career. He received his BSc (Hons) degree in Applied Geology from University of the Punjab, Lahore, Pakistan and MSc by Research degree in Geosciences from University Teknologi PETRONAS, Malaysia.

Professor Reza Rezaee of Curtin University’s Department of Petroleum Engineering has a PhD degree in Reservoir Characterisation. He has over 27 years’ experience in academia, being responsible for both teaching and research. During his career, he has been engaged in several research projects supported by major oil and gas companies. These commissions, together with his supervisory work at various universities, have involved a wide range of achievements. During his research career, he has led several major research projects funded by various oil and gas companies. He has published more than 160 peer-reviewed journal and conference papers and is the author of four books on petroleum geology, logging and log interpretation and gas shale reservoirs. His research has been mostly on integrated solutions for reservoir characterisation, formation evaluation and petrophysics. Currently, he is focused on unconventional gas, including gas shale and tight gas sand studies. As a founder of the ‘Unconventional Gas Research Group’ of Australia, he has established a unique and highly sophisticated research lab at the Department of Petroleum Engineering, Curtin University. This lab was established to conduct research on petrophysical evaluation of tight gas sands and shale gas formations. He is the winner of Australian Gas Innovation Award for his innovation on tight gas sand treatment for gas production enhancement.

Gregory Smith is Adjunct Professor of Petroleum Geology at Curtin University in the School of Earth and Planetary Sciences. He has over 40 years’ experience in petroleum geology, geophysics and geochemistry involving technical, research and managerial positions at Exxon, ARCO, BHP, Woodside/Shell and the Herman Research Laboratory. Initial research into 3D modelling of basins, sediments and organic geochemistry was followed by successful coal, oil shale and petroleum exploration. This included several major discoveries and field developments leading to production for many large projects in Australia and overseas. Greg undertakes research with Honours, Masters and PhD students on interpretation, organic geochemical and geostatistical analysis of large seismic, well log, core and production datasets. The results are used to build 3D structural and property models of sedimentary basins or petroleum fields, and analyses, using machine learning and multi factor scenario modelling, to estimate the probable geology and associated resource estimates. Specific interests include low temperature-pressure burial and thermal history modelling, organic matter petrology and geochemistry, and characterisation of sediments and their diagenesis with Curtin University departments of statistics and engineering, the WA Organic and Isotope Geochemistry group and the John de Laeter Centre. Greg is a member of AAPG, PESA, TSOP, ICCP, past corporate member of AusIMM, and has held various positions in GSA, PESA, APPEA and ASA.

Partha Pratim Mandal is a current PhD student at the WASM, Curtin University. His research focuses on creating geomechanical workflows to conduct laboratory measurements of the deformation aspect of shale gas, including the viscoelastic deformation, stress partitioning factor of rock composition, multi-channel active and passive wave velocity recording and elastic anisotropy. He is also interested in transferring geotechnical skill from the energy industry to the deep earth mining activity for safer operation. He is the recipient of several scholarships and research grants, such as the RTP Scholarship, EAGE Student Fund, PESA Federal Post-graduate Scholarship, AAPG Grant-in-Aid and the AIG Student Bursary Program. He was the founding member and the president of EAGE-SEG student chapter at Curtin University and currently serves as Secretary of the ASEG, WA branch. Previously, he worked for six years as the Imaging Geophysicist at PGS, both in India and Australia. He received his first-class BSc (Hons) degree in Physics from the Presidency College, University of Calcutta, India, and his MSc Tech degree in Applied Geophysics from the IIT (ISM), Dhanbad, India.


References

Ahmed, U. and Meehan, D. N. (2016). Unconventional oil and gas resources: exploitation and development, CRC Press

Arthur, M. A., and Sageman, B. B. (1994). Marine black shales: depositional mechanisms and environments of ancient deposits. Annual Review of Earth and Planetary Sciences 22, 499–551.
Marine black shales: depositional mechanisms and environments of ancient deposits.Crossref | GoogleScholarGoogle Scholar |

Brown, S., Boserio, I., Jackson, K. and Spence, K. (1984). The geological evolution of the Canning Basin-implications for petroleum exploration. In ‘The Canning Basin, WA’ Proceedings of Geological Society of Australia/Petroleum Exploration Society of Australia Symposium, Perth, 1984. (Ed Purcell, P.G.)

Brunauer, S., Emmett, P., and Teller, E. (1938). Absorption of gases in multimolecular layers. Journal of the American Chemical Society 60, 309–319.
Absorption of gases in multimolecular layers.Crossref | GoogleScholarGoogle Scholar |

Cabrera, L., and Saez, A. (1987). Coal deposition in carbonate-rich shallow lacustrine systems: the Calaf and Mequinenza sequences (Oligocene, eastern Ebro Basin, NE Spain). Journal of the Geological Society 144, 451–461.
Coal deposition in carbonate-rich shallow lacustrine systems: the Calaf and Mequinenza sequences (Oligocene, eastern Ebro Basin, NE Spain).Crossref | GoogleScholarGoogle Scholar |

Cadman, S., Pain, L., Vuckovic, V. and Le poidevin, S. (1993). Canning Basin. Western Australia: Australian Petroleum Accumulations Report 9, 81.

Chen, L., Jiang, Z., Liu, K., Wang, P., Ji, W., Gao, F., Li, P., Hu, T., Zhang, B., and Huang, H. (2016). Effect of lithofacies on gas storage capacity of marine and continental shales in the Sichuan Basin, China. Journal of Natural Gas Science and Engineering 36, 773–785.
Effect of lithofacies on gas storage capacity of marine and continental shales in the Sichuan Basin, China.Crossref | GoogleScholarGoogle Scholar |

Chen, L., Jiang, Z., Liu, K., Ji, W., Wang, P., Gao, F., and Hu, T. (2017). Application of Langmuir and Dubinin–Radushkevich models to estimate methane sorption capacity on two shale samples from the Upper Triassic Chang 7 Member in the southeastern Ordos Basin, China. Energy Exploration & Exploitation 35, 122–144.
Application of Langmuir and Dubinin–Radushkevich models to estimate methane sorption capacity on two shale samples from the Upper Triassic Chang 7 Member in the southeastern Ordos Basin, China.Crossref | GoogleScholarGoogle Scholar |

Curtis, J. B. (2002). Fractured shale-gas systems. AAPG Bulletin 86, 1921–1938.
Fractured shale-gas systems.Crossref | GoogleScholarGoogle Scholar |

Curtis, M. E., Sondergeld, C. H., Ambrose, R. J., and Rai, C. S. (2012). Microstructural investigation of gas shales in two and three dimensions using nanometer-scale resolution imagingMicrostructure of Gas Shales. AAPG Bulletin 96, 665–677.
Microstructural investigation of gas shales in two and three dimensions using nanometer-scale resolution imagingMicrostructure of Gas Shales.Crossref | GoogleScholarGoogle Scholar |

Ekundayo, J. M., and Rezaee, R. (2019). Effect of Equation of States on High-Pressure Volumetric Measurements of Methane–Coal Sorption Isotherms—Part 1: Volumes of Free Space and Methane Adsorption Isotherms. Energy & Fuels 33, 1029–1036.
Effect of Equation of States on High-Pressure Volumetric Measurements of Methane–Coal Sorption Isotherms—Part 1: Volumes of Free Space and Methane Adsorption Isotherms.Crossref | GoogleScholarGoogle Scholar |

Ferguson, D. P. (2016). The depositional history of the Ordovician lower Goldwyer Formation, Canning Basin, Western Australia. Master’s Thesis. The University of Western Australia.

Foster, C., O’brien, G., and Watson, S. (1986). Hydrocarbon source potential of the Goldwyer Formation, Barbwire Terrace, Canning Basin, Western Australia. The APPEA Journal 26, 142–155.
Hydrocarbon source potential of the Goldwyer Formation, Barbwire Terrace, Canning Basin, Western Australia.Crossref | GoogleScholarGoogle Scholar |

Haines, P. (2004). Depositional facies and regional correlations of the Ordovician Goldwyer and Nita Formations, Canning Basin, Western Australia, with implications for petroleum exploration. Geological Survey of Western Australia, Record , 7.

Iqbal, M. A., and Rezaee, R. (2020). Porosity and Water Saturation Estimation for Shale Reservoirs: An Example from Goldwyer Formation Shale, Canning Basin, Western Australia. Energies 13, 6294.
Porosity and Water Saturation Estimation for Shale Reservoirs: An Example from Goldwyer Formation Shale, Canning Basin, Western Australia.Crossref | GoogleScholarGoogle Scholar |

Iqbal, M. A., Rezaee, R., Smith, G., and Ekundayo, J. M. (2021). Shale lithofacies controls on porosity and pore structure: an example from Ordovician Goldwyer Formation, Canning Basin, Western Australia. Journal of Natural Gas Science and Engineering 89, 103888.
Shale lithofacies controls on porosity and pore structure: an example from Ordovician Goldwyer Formation, Canning Basin, Western Australia.Crossref | GoogleScholarGoogle Scholar |

Jarvie, D. M., Hill, R. J., Ruble, T. E., and Pollastro, R. M. (2007). Unconventional shale-gas systems: The Mississippian Barnett Shale of north-central Texas as one model for thermogenic shale-gas assessment. AAPG Bulletin 91, 475–499.
Unconventional shale-gas systems: The Mississippian Barnett Shale of north-central Texas as one model for thermogenic shale-gas assessment.Crossref | GoogleScholarGoogle Scholar |

Jing, T., Zhang, J., Mao, J., Li, W., and Jiang, S. (2014). Geological controls and mechanism of shale gas and shale oil accumulations in Liaohe western depression, China. Energy Exploration & Exploitation 32, 503–525.
Geological controls and mechanism of shale gas and shale oil accumulations in Liaohe western depression, China.Crossref | GoogleScholarGoogle Scholar |

Johnson, L. M. (2019). Integrated Reservoir Characterization of the Goldwyer Formation, Canning Basin. PhD Thesis. Curtin University. Available at http://hdl.handle.net/20.500.11937/77189.

Kadkhodaie, A., and Rezaee, R. (2016). A new correlation for water saturation calculation in gas shale reservoirs based on compensation of kerogen-clay conductivity. Journal of Petroleum Science and Engineering 146, 932–939.
A new correlation for water saturation calculation in gas shale reservoirs based on compensation of kerogen-clay conductivity.Crossref | GoogleScholarGoogle Scholar |

Labani, M. M., Rezaee, R., Saeedi, A., and Al hinai, A. (2013). Evaluation of pore size spectrum of gas shale reservoirs using low pressure nitrogen adsorption, gas expansion and mercury porosimetry: A case study from the Perth and Canning Basins, Western Australia. Journal of Petroleum Science and Engineering 112, 7–16.
Evaluation of pore size spectrum of gas shale reservoirs using low pressure nitrogen adsorption, gas expansion and mercury porosimetry: A case study from the Perth and Canning Basins, Western Australia.Crossref | GoogleScholarGoogle Scholar |

Liu, D., Li, Z., Jiang, Z., Zhang, C., Zhang, Z., Wang, J., Yang, D., Song, Y., and Luo, Q. (2019). Impact of laminae on pore structures of lacustrine shales in the southern Songliao Basin, NE China. Journal of Asian Earth Sciences 182, 103935.
Impact of laminae on pore structures of lacustrine shales in the southern Songliao Basin, NE China.Crossref | GoogleScholarGoogle Scholar |

Loucks, R. G., Reed, R. M., Ruppel, S. C., and Jarvie, D. M. (2009). Morphology, genesis, and distribution of nanometer-scale pores in siliceous mudstones of the Mississippian Barnett Shale. Journal of Sedimentary Research 79, 848–861.
Morphology, genesis, and distribution of nanometer-scale pores in siliceous mudstones of the Mississippian Barnett Shale.Crossref | GoogleScholarGoogle Scholar |

Martini, A. M., Walter, L. M., Ku, T. C., Budai, J. M., Mcintosh, J. C., and Schoell, M. (2003). Microbial production and modification of gases in sedimentary basins: A geochemical case study from a Devonian shale gas play, Michigan basin. AAPG Bulletin 87, 1355–1375.
Microbial production and modification of gases in sedimentary basins: A geochemical case study from a Devonian shale gas play, Michigan basin.Crossref | GoogleScholarGoogle Scholar |

Molinares, C., Slatt, R. and Sierra, R. (2016). Effect of anisotropy (lamination) on rock fracability for vertical transverse isotropic (VTI) unconventional reservoirs, a comparison between upper (Highstand system tract-HST) and middle (Transgressive system tract-TST) Woodford shale. SEG Technical Program Expanded Abstracts 2016. Society of Exploration Geophysicists.

Parra-Garcia, M., Sanchez, G., Dentith, M., and George, A. (2014). Regional structural and stratigraphic study of the Canning Basin. Western Australia: Perth, Western Australia, Australia, Geological Survey of Western Australia Report 140, 215.

Ravikovitch, P. I., Vishnyakov, A., Russo, R., and Neimark, A. V. (2000). Unified approach to pore size characterization of microporous carbonaceous materials from N2, Ar, and CO2 adsorption isotherms. Langmuir 16, 2311–2320.
Unified approach to pore size characterization of microporous carbonaceous materials from N2, Ar, and CO2 adsorption isotherms.Crossref | GoogleScholarGoogle Scholar |

Reilly, J. (1988). Synthesis of the tectonic and sedimentological evolution of the Canning Basin. Exploration Geophysics 19, 135–141.
Synthesis of the tectonic and sedimentological evolution of the Canning Basin.Crossref | GoogleScholarGoogle Scholar |

Rezaee, R. (2015). Fundamentals of gas shale reservoirs. John Wiley & Sons.

Ross, D. J. K., and Marc bustin, R. (2009). The importance of shale composition and pore structure upon gas storage potential of shale gas reservoirs. Marine and Petroleum Geology 26, 916–927.
The importance of shale composition and pore structure upon gas storage potential of shale gas reservoirs.Crossref | GoogleScholarGoogle Scholar |

Ross, D. A., Degens, E. T., and Macilvaine, J. (1970). Black Sea: recent sedimentary history. Science 170, 163–165.
Black Sea: recent sedimentary history.Crossref | GoogleScholarGoogle Scholar | 17833497PubMed |

Sun, T., Merletti, G., Patel, H., Cadwallader, S., Graff, M. C., Wampler, J., Gil, I. R., Sebastian, H., Spain, D. and Aguirre, O. (2015). Advanced petrophysical, geological, geophysical and geomechanical reservoir characterization-key to the successful implementation of a geo-engineered completion optimization program in the Eagle Ford shale. Unconventional Resources Technology Conference, San Antonio, Texas, 20–22 July 2015. Society of Exploration Geophysicists, American Association of Petroleum. pp. 694–703.

Tang, X., Jiang, Z., Jiang, S., Cheng, L., and Zhang, Y. (2017). Characteristics and origin of in-situ gas desorption of the Cambrian Shuijingtuo Formation shale gas reservoir in the Sichuan Basin, China. Fuel 187, 285–295.
Characteristics and origin of in-situ gas desorption of the Cambrian Shuijingtuo Formation shale gas reservoir in the Sichuan Basin, China.Crossref | GoogleScholarGoogle Scholar |

Thomsen, E. (1989). Seasonal variability in the production of Lower Cretaceous calcareous nannoplankton. Geology 17, 715–717.
Seasonal variability in the production of Lower Cretaceous calcareous nannoplankton.Crossref | GoogleScholarGoogle Scholar |

Van hattum, J., Bond, A., Jablonski, D., and Taylor-Walshe, R. (2019). Exploration of an unconventional petroleum resource through extensive core analysis and basin geology interpretation utilising play element methodology: the Lower Goldwyer Formation, onshore Canning Basin, Western Australia. The APPEA Journal 59, 464–481.
Exploration of an unconventional petroleum resource through extensive core analysis and basin geology interpretation utilising play element methodology: the Lower Goldwyer Formation, onshore Canning Basin, Western Australia.Crossref | GoogleScholarGoogle Scholar |

Winchester-Seeto, T., Foster, C., and O’leary, T. (2000). The environmental response of Middle Ordovician large organic walled microfossils from the Goldwyer and Nita Formations, Canning Basin, Western Australia. Review of Palaeobotany and Palynology 113, 197–212.
The environmental response of Middle Ordovician large organic walled microfossils from the Goldwyer and Nita Formations, Canning Basin, Western Australia.Crossref | GoogleScholarGoogle Scholar | 11164220PubMed |

Yan, J., Zhang, Q., and Gao, J. (1979). Adsorption and condensation-the surface and pore of solid. Science, Beijing , 118–124.

Yang, F., Xu, S., Hao, F., Hu, B., Zhang, B., Shu, Z., and Long, S. (2019). Petrophysical characteristics of shales with different lithofacies in Jiaoshiba area, Sichuan Basin, China: Implications for shale gas accumulation mechanism. Marine and Petroleum Geology 109, 394–407.
Petrophysical characteristics of shales with different lithofacies in Jiaoshiba area, Sichuan Basin, China: Implications for shale gas accumulation mechanism.Crossref | GoogleScholarGoogle Scholar |

Yuan, Y., Rezaee, R., Al-Khdheeawi, E. A., Hu, S.-Y., Verrall, M., Zou, J., and Liu, K. (2019). Impact of Composition on Pore Structure Properties in Shale: Implications for Micro-/Mesopore Volume and Surface Area Prediction. Energy & Fuels 33, 9619–9628.
Impact of Composition on Pore Structure Properties in Shale: Implications for Micro-/Mesopore Volume and Surface Area Prediction.Crossref | GoogleScholarGoogle Scholar |

Zhang, T., Ellis, G. S., Ruppel, S. C., Milliken, K., and Yang, R. (2012). Effect of organic-matter type and thermal maturity on methane adsorption in shale-gas systems. Organic Geochemistry 47, 120–131.
Effect of organic-matter type and thermal maturity on methane adsorption in shale-gas systems.Crossref | GoogleScholarGoogle Scholar |

Zhang, L., Lu, S., Jiang, S., Xiao, D., Chen, L., Liu, Y., Zhang, Y., Li, B., and Gong, C. (2018). Effect of Shale Lithofacies on Pore Structure of the Wufeng–Longmaxi Shale in Southeast Chongqing, China. Energy & Fuels 32, 6603–6618.
Effect of Shale Lithofacies on Pore Structure of the Wufeng–Longmaxi Shale in Southeast Chongqing, China.Crossref | GoogleScholarGoogle Scholar |

Zou, J., and Rezaee, R. (2019). A Prediction Model for Methane Adsorption Capacity in Shale Gas Reservoirs. Energies 12, 280.
A Prediction Model for Methane Adsorption Capacity in Shale Gas Reservoirs.Crossref | GoogleScholarGoogle Scholar |